{"created":"2023-07-25T10:35:48.218384+00:00","id":10874,"links":{},"metadata":{"_buckets":{"deposit":"dc344fef-a789-479b-a7a2-089a1b936ba0"},"_deposit":{"created_by":10,"id":"10874","owners":[10],"pid":{"revision_id":0,"type":"depid","value":"10874"},"status":"published"},"_oai":{"id":"oai:senshu-u.repo.nii.ac.jp:00010874","sets":["27:32:162:163:1260"]},"author_link":["4454"],"item_10002_biblio_info_7":{"attribute_name":"書誌情報","attribute_value_mlt":[{"bibliographicIssueDates":{"bibliographicIssueDate":"2020-03-05","bibliographicIssueDateType":"Issued"},"bibliographicPageEnd":"68","bibliographicPageStart":"63","bibliographicVolumeNumber":"51","bibliographic_titles":[{"bibliographic_title":"専修自然科学紀要"}]}]},"item_10002_creator_2":{"attribute_name":"作成者","attribute_type":"creator","attribute_value_mlt":[{"creatorNames":[{"creatorName":"Matsumoto, Kouzou"}],"nameIdentifiers":[{"nameIdentifier":"4454","nameIdentifierScheme":"WEKO"}]}]},"item_10002_description_25":{"attribute_name":"内容記述","attribute_value_mlt":[{"subitem_description":"The Balz-Schiemann reaction of 4-aminopyridine afforded 4-fluoropyridine (1) in 20% yield, but the special care was required because 1 was unstable under the aqueous conditions. Both the detailed reaction conditions and the appearance of the reaction mixture are reported in detail. The detailed experimental procedure for the isolation of 1 is also presented. Some comments for [1]H NMR spectrum of 1 are given.","subitem_description_type":"Other"}]},"item_10002_identifier_registration":{"attribute_name":"ID登録","attribute_value_mlt":[{"subitem_identifier_reg_text":"10.34360/00010860","subitem_identifier_reg_type":"JaLC"}]},"item_10002_publisher_26":{"attribute_name":"公開者","attribute_value_mlt":[{"subitem_publisher":"専修大学自然科学研究所"}]},"item_10002_source_id_28":{"attribute_name":"ISSN","attribute_value_mlt":[{"subitem_source_identifier":"0386-5827","subitem_source_identifier_type":"ISSN"}]},"item_10002_source_id_29":{"attribute_name":"書誌レコードID","attribute_value_mlt":[{"subitem_source_identifier":"AN00132417","subitem_source_identifier_type":"NCID"}]},"item_10002_version_type_20":{"attribute_name":"出版タイプ","attribute_value_mlt":[{"subitem_version_resource":"http://purl.org/coar/version/c_be7fb7dd8ff6fe43","subitem_version_type":"NA"}]},"item_files":{"attribute_name":"ファイル情報","attribute_type":"file","attribute_value_mlt":[{"accessrole":"open_date","date":[{"dateType":"Available","dateValue":"2020-06-03"}],"displaytype":"detail","filename":"3102_0051_09.pdf","filesize":[{"value":"583.5 kB"}],"format":"application/pdf","licensetype":"license_note","mimetype":"application/pdf","url":{"label":"3102_0051_09.pdf","url":"https://senshu-u.repo.nii.ac.jp/record/10874/files/3102_0051_09.pdf"},"version_id":"769c4686-5fa7-4294-8cd2-1350376d4b8b"}]},"item_keyword":{"attribute_name":"キーワード","attribute_value_mlt":[{"subitem_subject":"松本","subitem_subject_scheme":"Other"},{"subitem_subject":"幸三","subitem_subject_scheme":"Other"}]},"item_language":{"attribute_name":"言語","attribute_value_mlt":[{"subitem_language":"eng"}]},"item_resource_type":{"attribute_name":"資源タイプ","attribute_value_mlt":[{"resourcetype":"departmental bulletin paper","resourceuri":"http://purl.org/coar/resource_type/c_6501"}]},"item_title":"Detailed experimental procedure for the synthesis of 4-fluoropyridine","item_titles":{"attribute_name":"タイトル","attribute_value_mlt":[{"subitem_title":"Detailed experimental procedure for the synthesis of 4-fluoropyridine","subitem_title_language":"en"}]},"item_type_id":"10002","owner":"10","path":["1260"],"pubdate":{"attribute_name":"公開日","attribute_value":"2020-06-03"},"publish_date":"2020-06-03","publish_status":"0","recid":"10874","relation_version_is_last":true,"title":["Detailed experimental procedure for the synthesis of 4-fluoropyridine"],"weko_creator_id":"10","weko_shared_id":-1},"updated":"2023-07-25T12:14:24.834110+00:00"}